SEMQuant results. Listed at 1:29:07 AM on 2/3/00 Operator: Christie Rowe Client: none Job: Christie's Thesis Spectrum label: rmb4a-4f.txt Calibration data: Energy Resn. Area Strobe: -3.7 128.97 753068 Calib. element: 6921.1 183.94 75855 Gain factor = 99.991 Livetime = 50.0 seconds Sample data: Energy Resn. Area Strobe: -3.8 44.59 39144 Total spectrum counts = 137304 Livetime = 50.0 seconds System resolution = 49 eV Geometry (degrees): Tilt = 0.00 ED geometry (degrees): Elevation = 30.00 Azimuth = 0.00 Entry angle = 30.00 Accelerating voltage = 20.00 kV Quantitative method: ZAF ( 3 iterations). Analysed elements combined with: O ( Valency: -2) Method : Stoichiometry Nos. of ions calculation based on 23 anions per formula. 4 peaks possibly omitted: 0.05, 0.25, 0.51, 0.74 keV Standards : Na K Jd_CVG-9 12/30/99 Mg K Mg_EnJTC3 12/30/99 Al K Ca_AnJTC6 12/29/99 Si K Jd_CVG-9 12/30/99 P K P_ApSC3 12/30/99 K K K_OrCVG15 12/30/99 Ca K Ca_WoCVG6 12/30/99 Cr K Cr_ChrmSC4 12/30/99 Mn K Mn_RhoSC16 12/30/99 Fe K Fe_FaSC6 12/30/99 Elmt Spect. Fit Apparent Stat. k Ratio k Ratio Type Index Conc. Sigma Sigma Na K ED 0.6 4.322 0.084 0.38973 0.00762 Mg K ED 0.3 3.398 0.066 0.14148 0.00274 Al K ED 1.7 4.218 0.072 0.21742 0.00372 Si K ED 3.3 26.933 0.144 0.98405 0.00527 P K ED 1.2 -0.013* 0.037 -0.00072* 0.00208 K K ED 0.1 -0.017* 0.041 -0.00140* 0.00329 Ca K ED 0.2 0.696 0.047 0.02034 0.00137 Cr K ED 0.2 -0.016* 0.051 -0.00040* 0.00124 Mn K ED 0.9 0.106* 0.063 0.00316* 0.00187 Fe K ED 0.9 11.262 0.187 0.21447 0.00357 Elmt Spect. Inten. Std Element Sigma Atomic Compound Nos. of Type Corrn. Corrn. % % % % ions Na K ED 0.787 1.00 5.49 0.11 5.30 Na2O 7.40 2.02 Mg K ED 0.757 1.00 4.49 0.09 4.10 MgO 7.44 1.56 Al K ED 0.803 1.00 5.25 0.09 4.32 Al2O3 9.92 1.65 Si K ED 1.018 1.00 26.45 0.14 20.88 SiO2 56.57 7.98 P K ED 0.646 1.00 -0.02* 0.06 -0.01* P2O5 -0.05* -0.01* K K ED 1.001 1.00 -0.02* 0.04 -0.01* K2O -0.02* 0.00* Ca K ED 0.964 1.00 0.72 0.05 0.40 CaO 1.01 0.15 Cr K ED 0.941 1.00 -0.02* 0.05 -0.01* Cr2O3 -0.03* 0.00* Mn K ED 0.959 1.00 0.11* 0.07 0.04* MnO 0.14* 0.02* Fe K ED 0.930 1.00 12.11 0.20 4.81 FeO 15.58 1.84 O 43.42 0.24 60.19 23.00 Total 97.98 100.00 97.98 Cation sum 15.22 * = <2 Sigma Interpreted formula: Na2.02 Mg1.56 Al1.65 Ca0.15 Fe1.84 Si7.98 O23 Na2 Mg1.5 Al1.5 Ca.15 Fe1.85 Si8 O22 (OH)2 Glaucophane